Water → 3-Propylhexanimidic acid

HRID 1389833Notes

Reaction equation

[CH2:1]([CH:4]([CH2:8][CH2:9][CH3:10])[CH2:5][C:6]#[N:7])[CH2:2][CH3:3].[OH2:11]>>[CH2:1]([CH:4]([CH2:8][CH2:9][CH3:10])[CH2:5][C:6]([NH2:7])=[O:11])[CH2:2][CH3:3]

Participants

Reactant 2

HCID 962Water

HCID 179124003-Propylhexanenitrile

Product 1

HCID 30433043-Propylhexanimidic acid

Conditions

Temperature: 80 °C

Procedure

While stirring, 139.2 g (1 mol) of 3-n-propyl-hexanenitrile were added. The mixture was heated to 80° C. and maintained at this temperature for 2 hours. After cooling to room-temperature, the medium was hydrolysed while stirring with 1500 g of distilled water for 1 hour. The crude product so obtained was suction-filtered and taken up, while stirring for 1 hour at room-temperature, with 1500 g of distilled water. The medium was again suction-filtered, washed and dried to constant weight in a drying-oven under vacuum.

Workup

temperaturemaintained at this temperature for 2 hours
temperatureAfter cooling to room-temperature

Sources & evidence

ORD record: ord-8f7b8e67f8ca4a6b9225c45008c24018
Source dataset: uspto-grants-1981_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04246282

Reaction notes

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