Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Propylhexanenitrile | HCID 17912400 | — |
| Product | 3-Propylhexanimidic acid | HCID 3043304 | — |
Reaction Steps
While stirring, 139.2 g (1 mol) of 3-n-propyl-hexanenitrile were added. The mixture was heated to 80° C. and maintained at this temperature for 2 hours. After cooling to room-temperature, the medium was hydrolysed while stirring with 1500 g of distilled water for 1 hour. The crude product so obtained was suction-filtered and taken up, while stirring for 1 hour at room-temperature, with 1500 g of distilled water. The medium was again suction-filtered, washed and dried to constant weight in a drying-oven under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04246282 |
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| Source dataset | uspto-grants-1981_01 |
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| ORD ID | ord-8f7b8e67f8ca4a6b9225c45008c24018 |
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| Source note | uspto-grants-1981_01 |
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