Hydrochloric Acid → HCID 178458206, compound

HRID 1390018Notes

Reaction equation

HRID 1390018 reaction equation
[CH2:1]([N:3]([CH2:6][CH2:7][NH:8][C:9]1[C:14]([N+:15]([O-])=O)=[CH:13][CH:12]=[C:11]([O:18][CH2:19][CH2:20][CH3:21])[N:10]=1)[CH2:4][CH3:5])[CH3:2].Cl[C:23](OCC)=[O:24].Cl>>[CH2:1]([N:3]([CH2:4][CH3:5])[CH2:6][CH2:7][N:8]1[C:9]2[N:10]=[C:11]([O:18][CH2:19][CH2:20][CH3:21])[CH:12]=[CH:13][C:14]=2[N:15]=[C:23]1[OH:24])[CH3:2]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 10928Ethyl chloroformateHCID 54483063HCID 54483063, compound

Product 1

HCID 178458206HCID 178458206, compound

Procedure

The compound was produced in a manner analogous to Example 4 (or Example 5) starting from 36 grams of 2-(diethylaminoethylamino)-3-nitro-6-n-propoxypyridine and 13.5 grams of ethyl chloroformate produced. Yield: 24 grams M.P. of the hydrochloride 210°-212° C.

Workup

  1. customThe compound was produced in a manner analogous to Example 4 (or Example 5)
  2. customproduced

Sources & evidence

ORD record
ord-142b512e5544471dad18a1c833bbdd4a
Source dataset
uspto-grants-1981_01
Patent number
US04247556

Reaction notes

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