Hydrochloric Acid → HCID 178463988, compound

HRID 1390019Notes

Reaction equation

HRID 1390019 reaction equation
[CH2:1]([N:3]([CH2:16][CH3:17])[CH2:4][CH2:5][CH2:6][NH:7][C:8]1[C:13]([NH2:14])=[CH:12][CH:11]=[C:10]([Cl:15])[N:9]=1)[CH3:2].Cl[C:19](OCC)=[O:20].Cl>>[CH2:16]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][N:7]1[C:8]2[N:9]=[C:10]([Cl:15])[CH:11]=[CH:12][C:13]=2[N:14]=[C:19]1[OH:20])[CH3:17]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 10928Ethyl chloroformateHCID 20294681HCID 20294681, compound

Product 1

HCID 178463988HCID 178463988, compound

Procedure

The production was carried out in a manner analogous to Example 1 from 20 grams of 2-(3-diethylamino-propylamino)-3-amino-6-chloropyridine and 9 ml of ethyl chloroformate. M.P. of the hydrochloride of the title compound was 203°-205° C.; yield: 14 grams.

Sources & evidence

ORD record
ord-75d05398ed534e7a8ff27004ec81b69a
Source dataset
uspto-grants-1981_01
Patent number
US04247556

Reaction notes

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