Propane sultone → HCID 86737462, compound

Participants

Reaction Steps

In a mixture of 50 ml. of ethanol and 0.46 g. of metallic sodium were dissolved 3.4 g. of 2-mercapto-4-nitroaniline and 2.44 g. of propanesultone were added thereto under stirring. Thereafter, heating was conducted at 40°-50° C. for 1 hour and the crystalline substance thus separated was recovered by filtration, washed with ethanol and acetone and then dried to give 2 g. of the desired product. m.p. 181°-193° C.

Provenance & Evidence