HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodo-2-methoxyethane → HCID 86736278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodo-2-methoxyethane | HCID 79136 | — |
| Reactant | Bis(2-cyanoethyl)phenylphosphine | HCID 342156 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86736278 | HCID 86736278 | — |
Reaction Steps
8.5 g (0.04 mole) of bis-(β-cyanoethyl)-phenylphosphine are dissolved in 50 ml of absolute acetonitrile in a nitrogen atmosphere. Then 7.71 g (0.04 mole) of 1-iodo-2-methoxyethane are added and the mixture is refluxed for 12 hours. The solvent is distilled off to yield 13.2 g (82% of theory) of the product in the form of a solid, glassy substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138256 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-e2296da97d5744dbb5b864c042dcf026 |
| Source note | uspto-grants-1979_02 |