HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22748383, compound → HCID 22748363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22748383 | HCID 22748383 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22748363 | HCID 22748363 | — |
Reaction Steps
By dispersing 6.4 g of Intermediate 3 in 64 ml of ethanol and then hydrogenating the intermediate in an autoclave using a palladium-carbon catalyst, the desired product was obtained. The solvent used for the recrystallization was ethanol. The melting point of the product was 147-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138258 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-886693f544df4c5c9005bbb61954e989 |
| Source note | uspto-grants-1979_02 |