反应详情

All of the material produced in (g) was dissolved in methylene chloride (3 ml). To this solution was added AgBF4 (0.074 g) and Ag2O (0.44g). After stirring for 1/2 hour the suspension was filtered and the filtrate washed with NaHCO3 and water, dried and evaporated. Chromatography of the residue yielded the title compound (e17) (0.025 g), which was a mixture of the compound with the (2RS, 3SR, 5RS) stereochemistry and also the compound (2RS, 3SR, 5SR) stereochemistry in the ratio of 10:1.

1. filtrationwas filtered
2. washthe filtrate washed with NaHCO3 and water
3. customdried
4. customevaporated