HCID 22748561, compound → HCID 22748559, compound

Participants

Reaction Steps

All of the material produced in (g) was dissolved in methylene chloride (3 ml). To this solution was added AgBF4 (0.074 g) and Ag2O (0.44g). After stirring for 1/2 hour the suspension was filtered and the filtrate washed with NaHCO3 and water, dried and evaporated. Chromatography of the residue yielded the title compound (e17) (0.025 g), which was a mixture of the compound with the (2RS, 3SR, 5RS) stereochemistry and also the compound (2RS, 3SR, 5SR) stereochemistry in the ratio of 10:1.

Provenance & Evidence