HRID1390213

反应详情

EQUATION

反应方程式

HRID 1390213 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

The α-benzamido(2,3-dihydro-5-benzofuranyl)acetic acid (100 mg) is dissolved in 20 ml of methanol and 40 ml of water. Then 20 mg of Pd/C catalyst is added and the mixture subjected to 40 pounds/in2 of hydrogen pressure for 4 hours. The mixture is filtered to remove the solid and the methanol is evaporated to give the title compound in about 60% yield.

WORKUP

后处理

  1. customfor 4 hours
  2. filtrationThe mixture is filtered
  3. customto remove the solid
  4. customthe methanol is evaporated