HRID1390213
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The α-benzamido(2,3-dihydro-5-benzofuranyl)acetic acid (100 mg) is dissolved in 20 ml of methanol and 40 ml of water. Then 20 mg of Pd/C catalyst is added and the mixture subjected to 40 pounds/in2 of hydrogen pressure for 4 hours. The mixture is filtered to remove the solid and the methanol is evaporated to give the title compound in about 60% yield.
WORKUP
后处理
- customfor 4 hours
- filtrationThe mixture is filtered
- customto remove the solid
- customthe methanol is evaporated