HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → 2-Pyrazinyl-ethyl methyl sulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Vinylpyrazine | HCID 77840 | — |
| Product | 2-Pyrazinyl-ethyl methyl sulfide | HCID 22630400 | — |
Reaction Steps
h. 2-Pyrazinyl-ethyl methyl sulfide was prepared by reacting vinylpyrazine [c.f. J.Org.Chem. 27, 1363 (1962)] with methylmercaptan by the action of ultra-violet light and in the presence of benzoyl peroxide by the method described in Acta Chem. Scand. 8, 295 (1954). The product was identified by mass spectrometry. It has a b.p. of 57°-69° C. at 0.05 mm. Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138410 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-587579e4b01b4cafa8cc285ec83c174d |
| Source note | uspto-grants-1979_02 |