Vinyl Chloride → HCID 178527065, compound

HRID 1390255Notes

Reaction equation

HRID 1390255 reaction equation
C([Cl:3])=C.[Cl:4]Cl.[Cl-:6].[Cl-:7].[CH2:8]([O:11][P:12](=[O:15])(O)[OH:13])[CH2:9]C>>[Cl-:3].[Cl-:4].[Cl:6][CH:8]([O:11][PH:12](=[O:15])[OH:13])[CH2:9][Cl:7]

Participants

4

Reactant 3

HCID 6338Vinyl ChlorideHCID 24526ChlorineHCID 131711413HCID 131711413, compound

Product 1

HCID 178527065HCID 178527065, compound

Procedure

20 g of vinyl chloride and 20 g of chlorine are passed into 20 g of phosphoric acid monopropyl ester-dichloride, the reaction temperature being kept between 0° C. and +10° C. by cooling. Working up by the distillation gives 16g (=62.5% of theory) of phosphonic acid (1,2-dichloroethyl) ester-dichloride, which has a boiling range of 56° - 60° C./0.1 mm Hg.

Workup

  1. custombeing kept between 0° C. and +10° C.
  2. temperatureby cooling
  3. distillationWorking up by the distillation

Sources & evidence

ORD record
ord-9e7384b285224681882eb864c8bd8077
Source dataset
uspto-grants-1979_02
Patent number
US04138452

Reaction notes

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