Vinyl Chloride → HCID 178527065, compound

Participants

Reaction Steps

20 g of vinyl chloride and 20 g of chlorine are passed into 20 g of phosphoric acid monopropyl ester-dichloride, the reaction temperature being kept between 0° C. and +10° C. by cooling. Working up by the distillation gives 16g (=62.5% of theory) of phosphonic acid (1,2-dichloroethyl) ester-dichloride, which has a boiling range of 56° - 60° C./0.1 mm Hg.

Provenance & Evidence