HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70605513, compound → HCID 70604765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70605513 | HCID 70605513 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Potassium Carbonate | HCID 11430 | — |
| Product | HCID 70604765 | HCID 70604765 | — |
Reaction Steps
A solution of 5-androstene-3β,17β,19-triol triacetate in methanol and potassium carbonate in water is combined and stirred at room temperature for a period of about 2 hours. The solution is poured onto water and the solid which forms is collected by filtration. Crystallization of this solid from an acetone solution yields 5-androstene-3β,17β,19-triol 17-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04139617 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-68069eb63cbb4f9fa78e567fdaaf9c46 |
| Source note | uspto-grants-1979_02 |