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HRID1390819

反应详情

EQUATION

反应方程式

HRID 1390819 的结构方程式

REACTANTS

反应物

2
结构：N#CC(N)c1ccccc1
HCID40838

未命名化合物

结构：CCC(=O)CC(C)=O
HCID76355

2,4-Hexanedione

C6H10O2

PRODUCTS

生成物

1
结构：CCC(=O)c1c(C)[nH]c(-c2ccccc2)c1N
HCID20330040

1-(4-Amino-2-methyl-5-phenyl-1H-pyrrol-3-yl)-1-propanone

C14H16N2O

收率 53%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Starting from 2-amino-2-phenylacetonitrile and hexane-2,4-dione, the open-chain intermediate compound is obtained, b.p. 160° C./0.3 mm Hg. The title compound is obtained in an overall yield of 53%, m.p. 166°-168° C. (from methanol).

WORKUP

后处理

  1. customthe open-chain intermediate compound is obtained