Acetoacetanilide → HCID 14616662, compound

HRID 1390823Notes

Reaction equation

HRID 1390823 reaction equation
[NH2:1][CH:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[C:3]#[N:4].[C:11]([CH2:14][C:15]([NH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[O:16])(=O)[CH3:12]>C(O)C>[NH2:4][C:3]1[C:14]([C:15](=[O:16])[NH:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[C:11]([CH3:12])[NH:1][C:2]=1[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

4

Reactant 2

HCID 7592AcetoacetanilideHCID 408382-Amino-2-phenylacetonitrile

Product 1

HCID 14616662HCID 14616662, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

This compound is prepared starting from 2-amino-2-phenylacetonitrile and α-acetyl-N-phenyl-acetamide, and is obtained with a 73% overall yield, m.p. 271°-73° C. (from ethanol).

Workup

  1. customThis compound is prepared

Sources & evidence

ORD record
ord-0a74e708fddb4debacbca66bb9f9e0e5
Source dataset
uspto-grants-1979_02
Patent number
US04140696

Reaction notes

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