HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetoacetanilide → 3-Amino-5-methyl-2-phenyl-4-phenylcarbamoylpyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetoacetanilide | HCID 7592 | — |
| Reactant | 2-Amino-2-phenylacetonitrile | HCID 40838 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Amino-5-methyl-2-phenyl-4-phenylcarbamoylpyrrole | HCID 14616662 | — |
Reaction Steps
This compound is prepared starting from 2-amino-2-phenylacetonitrile and α-acetyl-N-phenyl-acetamide, and is obtained with a 73% overall yield, m.p. 271°-73° C. (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140696 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-0a74e708fddb4debacbca66bb9f9e0e5 |
| Source note | uspto-grants-1979_02 |