Methyl vinyl ether → Pyrocatechol bis-[(1-methoxy)-ethyl]-ether
Reaction equation
[CH3:1][O:2][CH:3]([O:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[OH:12])[CH3:4].[CH3:13][O:14][CH:15]=[CH2:16]>>[C:6]1([C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[OH:12])[OH:5].[CH3:13][O:14][CH:15]([O:5][CH:3]([O:2][CH3:1])[CH3:4])[CH3:16]Participants
3
Procedure
The reaction described under (a) is repeated but with twice the amount (128 parts by weight) of vinyl methyl ether. 122 parts by weight of a colorless oil is obtained having a boiling point of 99° to 105° C. at 0.5 mm.
Workup
- custom122 parts by weight of a colorless oil is obtained
Sources & evidence
- ORD record
- ord-16ef0f3050f34b858fb213977ef69eec
- Source dataset
- uspto-grants-1979_02
- Patent number
- US04140725
Reaction notes
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