Dimethylamine → HCID 12952391, compound

HRID 1390915Notes

Reaction equation

HRID 1390915 reaction equation
[C:1]([C:4]1[CH:5]=[CH:6][C:7](Cl)=[C:8]([S:10]([NH2:13])(=[O:12])=[O:11])[CH:9]=1)(=[O:3])[CH3:2].[CH3:15][NH:16][CH3:17]>C(O)C>[C:1]([C:4]1[CH:5]=[CH:6][C:7]([N:16]([CH3:17])[CH3:15])=[C:8]([S:10]([NH2:13])(=[O:12])=[O:11])[CH:9]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 126197985-Acetyl-2-chlorobenzene-1-sulfonamide

Product 1

HCID 12952391HCID 12952391, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

A mixture of 5-acetyl-2-chloro-benzenesulphonamide (0.5 g) in ethanol (10 ml) and dimethylamine in ethanol (33%, 5 ml) was heated in a closed vessel on a steam bath for 16 hours. The solvents were removed under reduced pressure and the residue crystallised from ethanol to give the product 0.31 g, m.p. 184°-185°.

Workup

  1. temperaturewas heated in a closed vessel on a steam bath for 16 hours
  2. customThe solvents were removed under reduced pressure
  3. customthe residue crystallised from ethanol

Sources & evidence

ORD record
ord-1549e093f701489f816a05493178400c
Source dataset
uspto-grants-1979_02
Patent number
US04140713

Reaction notes

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