HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 12952391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 5-Acetyl-2-chlorobenzene-1-sulfonamide | HCID 12619798 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12952391 | HCID 12952391 | — |
Reaction Steps
A mixture of 5-acetyl-2-chloro-benzenesulphonamide (0.5 g) in ethanol (10 ml) and dimethylamine in ethanol (33%, 5 ml) was heated in a closed vessel on a steam bath for 16 hours. The solvents were removed under reduced pressure and the residue crystallised from ethanol to give the product 0.31 g, m.p. 184°-185°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140713 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-1549e093f701489f816a05493178400c |
| Source note | uspto-grants-1979_02 |