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HRID1390919

反应详情

EQUATION

反应方程式

HRID 1390919 的结构方程式

REACTANTS

反应物

2
结构：N
HCID222

Ammonia gas

H3N

结构：CC(=O)c1ccc(F)c(S(N)(=O)=O)c1
HCID21331652

Benzenesulfonamide, 5-acetyl-2-fluoro-

C8H8FNO3S

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(N)c(S(N)(=O)=O)c1
HCID12952399

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

A solution of 5-acetyl-2-fluorobenzenesulphonamide (0.5 g) in ethanol (40 ml) saturated with ammonia was heated at 100° in a bomb overnight. Concentration of the resultant solution yielded a yellow crystalline solid, 0.4 g, m.p. 263°-264° (from ethanol).