HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-Acetyl-2-aminobenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Acetyl-2-fluorobenzenesulphonamide | HCID 21331652 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Acetyl-2-aminobenzenesulfonamide | HCID 12952399 | — |
Reaction Steps
A solution of 5-acetyl-2-fluorobenzenesulphonamide (0.5 g) in ethanol (40 ml) saturated with ammonia was heated at 100° in a bomb overnight. Concentration of the resultant solution yielded a yellow crystalline solid, 0.4 g, m.p. 263°-264° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140713 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-29fb6051b58f4d79a090e50d77968522 |
| Source note | uspto-grants-1979_02 |