Ethylamine → HCID 12952400, compound

HRID 1390921Notes

Reaction equation

HRID 1390921 reaction equation
[C:1]([C:4]1[CH:5]=[CH:6][C:7](F)=[C:8]([S:10]([NH2:13])(=[O:12])=[O:11])[CH:9]=1)(=[O:3])[CH3:2].[CH2:15]([NH2:17])[CH3:16]>C(O)C>[C:1]([C:4]1[CH:5]=[CH:6][C:7]([NH:17][CH2:15][CH3:16])=[C:8]([S:10]([NH2:13])(=[O:12])=[O:11])[CH:9]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 6341EthylamineHCID 213316525-Acetyl-2-fluorobenzenesulphonamide

Product 1

HCID 12952400HCID 12952400, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 5-acetyl-2-fluorobenzenesulphonamide (6.0 g) and ethylamine (70% solution in water, 25 ml) in absolute ethanol (100 ml) was heated at 100° for 16 hours in a bomb. The resulting yellow solution was evaporated to small volume to deposit the title compound as an off-white crystalline solid, 6.0 g, m.p. 201°-204° (from ethanol).

Workup

  1. customThe resulting yellow solution was evaporated to small volume

Sources & evidence

ORD record
ord-b7826d77612c4368b6b030d972c8aee5
Source dataset
uspto-grants-1979_02
Patent number
US04140713

Reaction notes

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