HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 12952400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 5-Acetyl-2-fluorobenzenesulphonamide | HCID 21331652 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12952400 | HCID 12952400 | — |
Reaction Steps
A solution of 5-acetyl-2-fluorobenzenesulphonamide (6.0 g) and ethylamine (70% solution in water, 25 ml) in absolute ethanol (100 ml) was heated at 100° for 16 hours in a bomb. The resulting yellow solution was evaporated to small volume to deposit the title compound as an off-white crystalline solid, 6.0 g, m.p. 201°-204° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140713 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-b7826d77612c4368b6b030d972c8aee5 |
| Source note | uspto-grants-1979_02 |