HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20306079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12747881 | HCID 12747881 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20306079 | HCID 20306079 | — |
Reaction Steps
6,7-Dichloro-2,3-dihydro-5-(2-thenoyl)-2-benzofuran carboxylic acid (3.4 g.; 0.01M.) is combined with 2 ml. thionyl chloride and 50 ml. benzene. After 2 hours at reflux the excess thionyl chloride and benzene are removed by distillation at 20 mmHg to give 6,7-dichloro-2,3-dihydro-5-(2-thenoyl)-2-benzofuran carboxylic acid chloride as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140776 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-89fd6a62f7a8442998d5267dcec6caf0 |
| Source note | uspto-grants-1979_02 |