Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 70524951 | HCID 70524951 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21332184 | HCID 21332184 | — |
Reaction Steps
A solution of 0.1 mole of 1,6-dimethyl-1H-(1)-benzothieno[3,2-c]pyrazol-3-amine and 30.0 g. of acetic anhydride in 180 ml. of tetrahydrofuran was heated under reflux for 1 hour. The reaction mixture was then cooled to 20° C. and the precipitate which formed was collected by filtration. Recrystallization from N,N-dimethyl formamide/water gave N-(1,6-dimethyl-1H-(1)benzothieno-[3,2-c]pyrazol-3-yl)acetamide, m.p. 253°-255° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04140785 |
|---|
| Source dataset | uspto-grants-1979_02 |
|---|
| ORD ID | ord-d09b710d913b467f8bd398355339f922 |
|---|
| Source note | uspto-grants-1979_02 |
|---|
