HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycolic Acid → N,N'-(1,6-hexylene)-bis[2-hydroxyundecylamine] diglycolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycolic Acid | HCID 757 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1,6-Hexylene-bis[2-hydroxyundecylamine] | HCID 21332347 | — |
| Product | N,N'-(1,6-hexylene)-bis[2-hydroxyundecylamine] diglycolate | HCID 86734722 | — |
Reaction Steps
A solution of N,N'-(1,6-hexylene-bis[2-hydroxyundecylamine] (5 g.), glycolic acid (1.66 g.) and methanol was heated until the solids dissolved, then evaporated to dryness. Recrystallization of the solid from acetone afforded N,N'-(1,6-hexylene)bis[2-hydroxyundecylamine] diglycolate (4.6 g., m.p. 88.2°-94.6° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140860 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-acf8e565aedb4f45ba87308302744d0a |
| Source note | uspto-grants-1979_02 |