HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 178465508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | HCID 178420865 | HCID 178420865 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178465508 | HCID 178465508 | — |
Reaction Steps
A solution of 1.85 g of 4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine and 2 g of ethyl isothiocyanate in 15 ml of acetonitrile are refluxed for 7 h. The solution is cooled and filtered: 2.5 g of 5-[N-ethyl-thiocarbamoyl]-4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine, m.p. 185°, are collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141899 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-a6e00b8e4b894491b68e41761719e065 |
| Source note | uspto-grants-1979_02 |