HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178512450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Methyl-2-thiopseudourea | HCID 5142 | — |
| Reactant | HCID 178420865 | HCID 178420865 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178512450 | HCID 178512450 | — |
Reaction Steps
A solution of 1.23 g of 4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine and 0.9 g of S-methyl-isothiourea in 15 ml of acetonitrile is refluxed for 8 h. After evaporation to dryness, the residue is treated with one equivalent of ethanolic hydrogen chloride. After cooling, 1.4 g of 5-guanyl-4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine monohydrochloride, m.p. 310°, are collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141899 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-bab96641c1384480a372c3bbd31b5d5a |
| Source note | uspto-grants-1979_02 |