HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl Isothiocyanate → HCID 23342288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl Isothiocyanate | HCID 75263 | — |
| Reactant | HCID 21330749 | HCID 21330749 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 23342288 | HCID 23342288 | — |
Reaction Steps
A solution of 9.3 g of 3,4-diethyl-4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine and 7.59 g of isopropyl isothiocyanate in 75 ml of anhydrous CH3CN is refluxed for 7.5 hours. The solution is allowed to stand overnight at -15° C., then is filtered. 5.59 g of the crude title compound are collected; m.p. 195° C. (recrystallized from CH3CN).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141899 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-68425a3173ca4342a415f05cf6059307 |
| Source note | uspto-grants-1979_02 |