HuagongsheHuagongshe Chemistry Print Report · For research reference only
Red-Al → HCID 70608796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Red-Al | HCID 16684438 | — |
| Reactant | HCID 70608295 | HCID 70608295 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 70608796 | HCID 70608796 | — |
Reaction Steps
Following the procedure set out in Example 7, dl-trans-1-oxo-2-methyl-5a-(3-methoxyphenyl)-decahydrocyclopent[c]azepine was reacted with Red-al® in benzene to provide dl-trans-2-methyl-5a-(3-methoxyphenyl)-decahydrocyclopent[c]azepine. B.P. 130°-140° C. at 0.05 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141893 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-588b1d4ed0d24637b54167e56dd29c4e |
| Source note | uspto-grants-1979_02 |