HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibromoacetyl chloride → HCID 21330776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibromoacetyl chloride | HCID 79184 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 21330784 | HCID 21330784 | — |
| Product | HCID 21330776 | HCID 21330776 | — |
Reaction Steps
In the manner given in Example 2, 7-fluoro-5-(o-chlorophenyl)-3H-1,4-benzodiazepin-2-yl hydrazine was reacted with dibromoacetyl chloride and after 1.5 hours with sodium acetate, then the mixture was refluxed to give 8-fluoro-1-(dibromomethyl)-6-(o-chlorophenyl)-4H-s-triazolo-[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141902 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-16bbf28ec13e4be1a6c13e3aeaa386ac |
| Source note | uspto-grants-1979_02 |