HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloroacetyl chloride → HCID 21330782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloroacetyl chloride | HCID 6593 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 21330777 | HCID 21330777 | — |
| Product | HCID 21330782 | HCID 21330782 | — |
Reaction Steps
In the manner given in Example 1, 6-trifluoromethyl-8-propylsulfonyl-5-(p-ethoxyphenyl)-3H-1,4-benzodiazepin-2-yl hydrazine was reacted with dichloroacetyl chloride and after 1.5 hours with sodium acetate, then refluxed to give 1-(dichloromethyl)-7-trifluoromethyl-9-propylsulfonyl-6-(p-ethoxyphenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141902 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-9ac280d6e8f041b5811f0291d403f99b |
| Source note | uspto-grants-1979_02 |