HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 136227082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | (4-Ethyl-2-hydroxyphenyl)(4-fluorophenyl)methanone | HCID 12562657 | — |
| Product | HCID 136227082 | HCID 136227082 | — |
Reaction Steps
4-Ethyl-4'-fluoro-2-hydroxybenzophenone (21.0 g, 80% pure) was treated with hydroxylamine hydrochloride (24.0 g) in a manner similar to that in Example 3, to give, after recrystallisation from benzene, the title compound as a white crystalline solid (10.7 g), m.p. 130°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141995 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-f5798c2b2b0444e2b3b9151ea5c8cfa6 |
| Source note | uspto-grants-1979_02 |