HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-benzyl-1H-indole-3-carbaldehyde → HCID 4637679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-benzyl-1H-indole-3-carbaldehyde | HCID 262104 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | HCID 4637679 | HCID 4637679 | 60% |
Reaction Steps
1-Benzyl-1H-indole-3-carbaldehyde oxime (1.752 g, 60%) was prepared from 1-benzyl-1H-indole-3-carbaldehyde and hydroxylamine hydrochloride using a procedure similar to Step 6 of example 1. 1H NMR (400 MHz, DMSO-d6); δ 11.30 (s, 1H), 8.40 (s, 1H), 7.88 (d, 1H), 7.80 (s, 1H), 7.50 (d, 1H), 7.22 (m, 7H), 5.50 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342039B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-c1e1fc4cd680475d866f9b1f490e2d85 |
| Source note | uspto-grants-2008_03 |