HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bromine → 2-Bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bromine | HCID 24408 | — |
| Edukt | 2-(4-Bromophenyl)-1-(2,4-dichlorophenyl)ethanone | HCID 63492363 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 2-Bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone | HCID 87768531 | 94% |
Reaktionsschritte
Part C: To a solution of 2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone (5.00 gram, 15 mmol) in benzene (50 mL) is dropwise added bromine (0.75 mL, 15 mmol) and the resulting solution is stirred for 4 hours at room temperature and concentrated in vacuo. Dichloromethane is added and the resulting solution is washed with brine, dried over MgSO4, filtered and concentrated in vacuo to give 2-bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone as an oil (5.96 gram, 94% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07342032B2 |
| Quelldatensatz | uspto-grants-2008_03 |
| ORD ID | ord-dcc3e75750d04b3e984e9e90539535f3 |
| Quellennotiz | uspto-grants-2008_03 |