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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1392366Erstellt: 26. Oktober 2026

Bromine → 2-Bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone

https://huagongshe.com/reaction/1392366

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBromineHCID 24408—
Edukt2-(4-Bromophenyl)-1-(2,4-dichlorophenyl)ethanoneHCID 63492363—
LösungsmittelBenzeneHCID 241—
Produkt2-Bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanoneHCID 8776853194%

Reaktionsschritte

Part C: To a solution of 2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone (5.00 gram, 15 mmol) in benzene (50 mL) is dropwise added bromine (0.75 mL, 15 mmol) and the resulting solution is stirred for 4 hours at room temperature and concentrated in vacuo. Dichloromethane is added and the resulting solution is washed with brine, dried over MgSO4, filtered and concentrated in vacuo to give 2-bromo-2-(4-bromophenyl)-1-(2,4-dichlorophenyl)ethanone as an oil (5.96 gram, 94% yield).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07342032B2
Quelldatensatzuspto-grants-2008_03
ORD IDord-dcc3e75750d04b3e984e9e90539535f3
Quellennotizuspto-grants-2008_03