HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10028870, compound → HCID 69310090, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10028870 | HCID 10028870 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 69310090 | HCID 69310090 | — |
Reaction Steps
50 ml of saturated hydrogenchloride-ethyl acetate solution was added to 4-[N-[1-[N-(pyridin-2-ylcarbonyl)amino]cyclohexanecarbonyl]amino]-1-(2-methanesulfonylphenyl)piperidin-3-one (500 mg) obtained in Example 144. The reaction mixture was stirred for 2 hours at room temperature and filtered to give 410 mg of the titled compound as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342027B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-a20af432622d440080a4eefa31c2ac41 |
| Source note | uspto-grants-2008_03 |