Hydrogen chloride-ethyl acetate → HCID 69311771, compound

Participants

Reaction Steps

50 ml of saturated hydrogenchloride-ethyl acetate solution was added to 4-[N-[1-[N-(4-(dimethylamino)benzoyl)amino]cyclohexanecarbonyl]amino]-1-(4-fluoro-2-methanesulfonylphenyl)piperidin-3-one (500 mg) obtained in Example 171. The reaction mixture was stirred for 2 hours at room temperature and filtered to give 250 mg of the titled compound as white solid.

Provenance & Evidence