HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl bromoacetate → Methyl (4-nitro-1-imidazolyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | HCID 178526856 | HCID 178526856 | — |
| Product | Methyl (4-nitro-1-imidazolyl)acetate | HCID 3103698 | — |
Reaction Steps
4-nitroimidazole was alkylated with bromo-acetic acid methyl ester to provide the title compound: 1H NMR (400 MHz) 3.82 (s, 1H), 4.80, (s, 2H), 7.47 (d, 1H, J=1.7 Hz), 7.84 (d, 1H, J=1.7 Hz); gc/ms m/z 185 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342118B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-29b34441757645559e47a6f66061c98b |
| Source note | uspto-grants-2008_03 |