HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-chloro-4-(methoxymethyl)benzene → 4-Chlorobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-chloro-4-(methoxymethyl)benzene | HCID 11983955 | — |
| Reactant | Sodium Bromate | HCID 23668195 | — |
| Product | 4-Chlorobenzaldehyde | HCID 7726 | — |
Reaction Steps
In the same manner as in Example 3, the operation was conducted, except that 0.63 g (4 mmols) of p-chlorobenzyl methyl ether was used in place of m-methoxybenzyl alcohol and also 0.2 g (1.35 mmols) of sodium bromate was used. With respect to the components in the reaction solution, the intended p-chlorobenzaldehyde was produced in an area ratio, as determined by gas chromatography, of 91.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342138B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-ed53b7f4aecc46c0ae8e15917403dc14 |
| Source note | uspto-grants-2008_03 |