HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 91584406, compound → HCID 10098111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 91584406 | HCID 91584406 | — |
| Solvent | HCID 131726520 | HCID 131726520 | — |
| Product | HCID 10098111 | HCID 10098111 | — |
Reaction Steps
The ester from step 3 (1 eq) in CH2Cl2-TFA-DMS (3:2:1, 0.2M) was stirred at rt for 48 h. The volatiles were evaporated, the residue triturated in ether and then isolated by filtration to afford the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342024B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-f4043f15cc57477a9f9de95999d00780 |
| Source note | uspto-grants-2008_03 |