HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 69310778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 69314748 | HCID 69314748 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69310778 | HCID 69310778 | — |
Reaction Steps
To a solution of the product of step g) (0.5 g) in methanol (10 ml) was added potassium carbonate (0.5 g) and the resulting suspension was stirred at ambient temperature for 2 hours. The reaction mixture was absorbed onto silica and purified by chromatography (SiO2; 3:1 isohexane:ethyl acetate) to give the subtitle compound (0.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345047B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-37ba9b618384441c923196a26b2272a8 |
| Source note | uspto-grants-2008_03 |