HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 56660575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 67424147 | HCID 67424147 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 56660575 | HCID 56660575 | 88.5% |
Reaction Steps
Using the procedure of Example 1B but replacing the resultant compound of Example 1A (Compound 1A-a) with the resultant compound of Example 1A(Compound 1A-b), provided, after silica gel chromatography using 5% methanol and 0.5% ammonium hydroxide in dichloromethane, 102.0 mg (88.5%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345034B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-ae24790b24b3482daf8313f47f8d64b3 |
| Source note | uspto-grants-2008_03 |