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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1393001Generated: November 3, 2026

Methanol → HCID 56660575, compound

https://huagongshe.com/reaction/1393001

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantAmmonium HydroxideHCID 14923—
ReactantHCID 67424147HCID 67424147—
SolventDichloromethaneHCID 6344—
ProductHCID 56660575HCID 5666057588.5%

Reaction Steps

Using the procedure of Example 1B but replacing the resultant compound of Example 1A (Compound 1A-a) with the resultant compound of Example 1A(Compound 1A-b), provided, after silica gel chromatography using 5% methanol and 0.5% ammonium hydroxide in dichloromethane, 102.0 mg (88.5%) of the title compound as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07345034B2
Source datasetuspto-grants-2008_03
ORD IDord-ae24790b24b3482daf8313f47f8d64b3
Source noteuspto-grants-2008_03