Hydrochloric Acid → HCID 69203826, compound

HRID 1393057Notes

Reaction equation

HRID 1393057 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([O:10]C)=[O:9])[CH3:3].[ClH:18]>>[ClH:18].[CH3:3][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([OH:10])=[O:9])[CH3:1]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 23144875HCID 23144875, compound

Product 1

HCID 69203826HCID 69203826, compound

Conditions

Temperature
100 °C

Procedure

The mixture of methyl 3-dimethylaminomethyl-2-nitrobenzoate (0.72 g) and 6M hydrochloric acid was stirred at 100° C. overnight. After cooling the mixture to room temperature, the precipitated crystals were filtered out, washed with diethylether and dried under reduced pressure to obtain 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride.

Workup

  1. temperatureAfter cooling the mixture to room temperature
  2. filtrationthe precipitated crystals were filtered out
  3. washwashed with diethylether
  4. customdried under reduced pressure

Sources & evidence

ORD record
ord-86c0a1d8138449b88f5963e6dbc7ac35
Source dataset
uspto-grants-2008_03
Patent number
US07345049B2

Reaction notes

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