2-Hydrazinoethanol → HCID 16045236, compound

HRID 1393239Notes

Reaction equation

HRID 1393239 reaction equation
[OH:1][CH2:2][CH2:3][NH:4][NH2:5].[Cl:6][C:7]1[CH:12]=[CH:11][C:10]([S:13]([N:16]2[CH:21]3[CH2:22][CH2:23][CH2:24][CH:17]2[C:18](=[CH:26]O)[C:19](=O)[CH2:20]3)(=[O:15])=[O:14])=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:8]=[CH:9][C:10]([S:13]([N:16]2[CH:21]3[CH2:22][CH2:23][CH2:24][CH:17]2[C:18]2[CH:26]=[N:5][N:4]([CH2:3][CH2:2][OH:1])[C:19]=2[CH2:20]3)(=[O:15])=[O:14])=[CH:11][CH:12]=1

Participants

3

Reactant 2

HCID 80172-HydrazinoethanolHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 16045236HCID 16045236, compound

Procedure

Prepared as described in Example 5 using hydroxyethylhydrazine and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-1816047c3b94415592eb9a88ba1548ee
Source dataset
uspto-grants-2008_03
Patent number
US07345056B2

Reaction notes

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