Hydroxyamine hydrochloride → HCID 16045473, compound
Reaction equation
Cl.O[NH2:3].[Cl:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([N:14]2[CH:19]3[CH2:20][CH2:21][CH2:22][CH:15]2[C:16](=[CH:24]O)[C:17](=[O:23])[CH2:18]3)(=[O:13])=[O:12])=[CH:7][CH:6]=1>>[Cl:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([N:14]2[CH:19]3[CH2:20][CH2:21][CH2:22][CH:15]2[C:16]2[CH:24]=[N:3][O:23][C:17]=2[CH2:18]3)(=[O:13])=[O:12])=[CH:7][CH:6]=1Participants
3
Procedure
Prepared as described in Example 5 using hydroxyamine hydrochloride and 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34.
Workup
- customPrepared
- customwas prepared
Sources & evidence
- ORD record
- ord-f37328a029964acaa435a916e8a483fc
- Source dataset
- uspto-grants-2008_03
- Patent number
- US07345056B2
Reaction notes
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