HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 23033855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 23033935 | HCID 23033935 | — |
| Product | HCID 23033855 | HCID 23033855 | 54% |
Reaction Steps
Methyl ester of 2-(2-dimethylaminopyrimidin-5-yl)benzoxazole-7-carboxylic acid (480 mg, 1.61 mmol) was reduced by using lithium aluminium hydride as in Preparation 2-3) to give 2-(2-dimethylamino-pyrimidin-5-yl)benzoxazole-7-methanol (234 mg, 54%) as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345068B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-40417fc9df8b435992afd23479810145 |
| Source note | uspto-grants-2008_03 |