HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10300899, compound → HCID 10136601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10300899 | HCID 10300899 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10136601 | HCID 10136601 | — |
Reaction Steps
23 mg of N-(phenylmethoxy)-6-[(1,2-diphenyl-1H-benzimidazol-6-yl)oxy]hexanamide was dissolved in 4 ml of ethanol, mixed with 15 mg of palladium on carbon (10%) and stirred under a hydrogen atmosphere for 3 hours. After catalyst was separated out, it was concentrated by evaporation in a vacuum, and the residue was crystallized from diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345075B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-97b3d7cc11374dc4b2b78dad5e66cbcd |
| Source note | uspto-grants-2008_03 |