HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67366246, compound → HCID 67364124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67366246 | HCID 67366246 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67364124 | HCID 67364124 | — |
Reaction Steps
340 mg of 6-[(1,2-diphenyl-7-nitro-1H-benzimidazol-6-yl)oxy]hexanoic acid methyl ester was hydrogenated in ethanol with Raney nickel in an autoclave at 50° C. and at normal pressure. After hydrogen absorption ended, catalyst was filtered out and concentrated by evaporation in a vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345075B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-6a30ebbb262449b387d0b77d14dcc449 |
| Source note | uspto-grants-2008_03 |