HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 10272450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 21938042 | HCID 21938042 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10272450 | HCID 10272450 | — |
Reaction Steps
35 mg of 2-[2-[(1,2-diphenyl-1H-benzimidazol-6-yl)oxy]ethoxy]acetic acid was dissolved in 0.4 ml of N,N-dimethylformamide and mixed with 29 mg of cesium carbonate and 50 μl of methyl iodide. It was stirred for 20 hours, then concentrated by evaporation in a vacuum and chromatographed on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345075B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-9bc1690be3154cb0bff16e02c4db285c |
| Source note | uspto-grants-2008_03 |